1.（福州）----______ Mary ______ Alice has joined the music club because they have no time.
         ----It’s a pity !
  A. Both…and     B. Either…or    C. Neither…nor
2.(重庆市) John, work hard _____ you will make much progress.
  A. or     B. nor       C. but       D. and
3. (滨州) ----What was your brother doing at this time yesterday ?
        ----He was reading a magazine ______ I was writing an email at home.
  A. as soon as            B. after             C. until         D. while
4.(山东菏泽) Stephen Hawking can’t walk or even speak，_____he has become very successful.
  A. but                 B. and              C. or           D. then
5.(杭州) I really enjoyed your lecture, ______ there were some parts I didn’t quite understand.
  A. because              B. unless           C. though        D. after
6.(杭州）It’s too late to invite any more people. _____, you know how Tom hates parties.
  A. Besides              B. However          C. Still          D. Instead
7.(宁波) ----I hear the famous singer Xu Rong may come to Ningbo next month.
       ----Really ? ______ he comes, my younger sister will be very excited.
  A. If                    B. Until             C. Unless        D. Before
8.(聊城) ----How do you like the story ?
       ----Interesting, _____ end of it is not perfect.
  A. so                    B. though            C. or           D. because
9.(烟台) _____ you have tried it on, you can’t imagined how pretty the new style skirt is.
  A. Because               B. Although          C. Unless       D. When
10.(南宁) Please hurry up, ______ you'll be late for school.
  A, but                    B. and               C. or          D. so
11.( 南京市) He was riding to school ______ he was hit by a car this morning.
  A. while                  B. when              C. as          D. so
12. (威海) ----Would you like to go for a walk with me , Allen ?
         ---- I’d love to , ______ you don’t want to go alone.
  A. until               B. before           C. if           D. after
13.(安徽) My father was preparing for his speech ______ my mother was doing some washing last night.
  A. if                  B. while               C. unless             D. until
14. (安徽) You'd better take the map with you ________you won't get lost,
  A. as long as         B. as soon as         C. now that          D. so that
15. (上海)Bob spends a lot of money on books _____ he is not rich.
  A. if          B. though           C. when           D. because
16.(江西) Mr. Smith comes from Australia , but he has worked in China for 5 years. So you can talk with him ________.
  A. either in English or in Chinese     B. not in Chinese but in English
  C. just in English , but not in Chinese  D. neither in Chinese nor in English
17.(泰安) ---Mom, shall we have supper now ?
        ---Oh, we won’t have supper _____your dad comes back.
  A. until         B. since         C. while        D. after
18.(兰州) Keep off the drugs, _____ you and your family will be in great danger.
  A. and           B. or             C. but           D. so
19.(济南) _______ our football team failed in the match, we did our best.
  A. Though        B. But            C. Because       D. As
20.(贵州铜仁) Neither my father nor my mother ________ rock music. They think that it’s too ______.
  A. like; noise    B. likes; noise         C. like; noisy   D. likes; noisy
21.(湖南邵阳) We didn’t go home _____ the old man was sent to the hospital.
  A. until               B. when            C. while
22.(四川德阳) _____ he was only twelve, he could run faster than any kids in the school.
  A. Though   B. Because   C. If
23. (浙江台州) I’ still remember my first teacher _____ we haven’t seen each other for a long time.
  A. if                 B. until              C. though        D. because
24.(浙江绍兴) ----I think your father is very busy .
            ----So he is. _____ he still takes a walk with us sometimes.
  A. So                B. And              C. or            D. But
25.(枣庄） I won’t pass the exam ______I work hard..
  A. whenever          B. because            C. if            D. unless
26.(济宁) Stand over there, ______ you will get a better view of the whole city.
  A. or                      B. and                     C. but             D. though
27.(广州) The little boy ate a big meal _______he said he wasn't hungry.
  A. if                B. though               C. because    D. as
28.(广州) —What do you like doing after class?
—I like not only reading ______painting.
  A. and              B. but also           C. or           D. for
29.(武汉) ----Where is Leo? He said he would come tonight!
----Yes, he did say so, _______we can’t find him now.
  A. and                B. so                C. but         D. or
30.(长沙) Mr. Black is rich, ________ he is not happy.
  A. and             B. or                C. but               D. 不填

参考答案：
1~5: CDDAC 6~10: AABCC 11~15: BCBDB 16~20: AABAD  21~25: ACCDD 26~30: BBBCC